Standardisation, Measurement, and Process Control

Today it is accepted that component parts for machinery are interchangeable without any adjustment. However, this was not always the case. For example, before the 1800’s firearms were made locally – muskets were individually handmade by specialist regional blacksmiths. This meant that parts from one musket were not interchangeable with another. There were no manufacturing standards or tolerance specifications or accurate gauges for checking dimensions.

It was not until later, driven by political and military needs, that techniques were developed to manufacture interchangeable parts for muskets and to inspect and test the parts to ensure uniformity.

Machine component parts are many and varied. Fasteners for example, based on the screw thread principle are common and screw thread history can be traced back to around 400 BC. Essentially, a screw mechanism is so useful because it converts and amplifies rotational movement into linear movement or force utilising mechanical advantage.

The wooden screw was widely used through the centuries for such things as olive oil and juice extraction presses and eventually metal screw fasteners appeared in the 15th century – but the threads were all handmade, different and non-standard. Due to the popularity of screw fasteners, there was always great demand and so it was necessary to speed up the production process. This came in the 1770’s when the screw cutting lathe was invented and production was radically increased by its use. A standard thread design though, was only introduced in the 1840’s by Joseph Whitworth. He standardised the thread pitch and angle and the Whitworth (BSW) thread became the world’s first ever national standard.

With continued industrialisation and the onset of the Industrial Revolution, it was not until the introduction of new machine tools and new machining techniques, that the technology to produce interchangeable parts made modern mass production and process control possible.

Industrialisation, infrastructure, commerce and cultural development drove this standardisation requirement. It extended in parallel to include other contemporary mechanical, communication and scientific needs, for example:

  • Units of weight and measurement
  • Currency
  • Gold standard
  • Time
  • Railways

These each have interesting histories and they all facilitate economies of scale in manufacturing and promote interoperability between complementary products and services.

Such standardization is a process that, if successful, creates a standard that is both authoritative and trusted. In many cases, the production of trusted knowledge occurs from using precision instruments for exact measurement.

In the early 20th century, the process of mass production evolved in car manufacturing – popularised by the Ford Motor Company, and the automotive and aerospace industries quickly became leading technological marketplaces with more standardisation, quality assurance and statistical process control needs.

The first standards organisation, the BSI was founded as the Engineering Standards Committee in London in 1901 and was followed by other organisations in other countries. These bodies produced standardised specifications, guidelines and codes of practice to enable industry and institutions to collaborate with uniformity.

In post WWII Germany, when the automotive industry was recovering from the war, Mr. Helmut Fischer developed an instrument that could quickly and precisely measure the thickness of paint and chrome coatings.

These coatings were applied to automotive components for protective and decorative purposes. Precise thicknesses needed to be achieved to ensure the correct mechanical and chemical properties of the coated components and to minimise the amount of coating material used. Fischer’s new instrumentation, in conjunction with Fischer calibration standard accessories, made this possible.

Among Fischer’s first customers were Bosch and Daimler and the company Fischer Instrumentation was created. It began supplying measurement solutions to the German automotive industry and grew quickly into a trusted instrument manufacturer and measurement authority wherever accuracy, precision and reliability were required.

With continued globalization, convergence and supply chain demands, Fischer continues today in the same tradition of pioneering, innovating and manufacturing precision instruments for measurement, testing and ensuring compliance to international standards. Across the globe, industry, research institutions and science depend on the accuracy and reliability of this equipment.

The new industrial revolution has now begun, and Fischer shapes technology and innovates new products including automated solutions for precision measurement, process control and calibration standards for manufacturing, R & D and testing industries into the 21st century.

Fischer Instrumentation (GB) Ltd

Measurement Made Easy

Measure Chrome/Nickel Coatings on Plastic Substrates

Coating Thickness and Elemental Composition Analysis of Multilayer-Coatings

Bathroom fittings are commonly finished with decorative chromium plating. But what may appear to be a solid metal shower head, for example, is often just a multi-layered metal coating on top of a plastic substrate. To guarantee that the showerhead not only looks pretty when delivered but even after many years of usage, the thickness of each individual layer must be controlled to ensure quality.

The typical composition of such shower heads is a chrome/nickel/copper coating system on top of plastic substrate material. The decorative chromium outer finish is usually only 0.5µm thick (or less) and the nickel layer is about 5-10µm. If the copper layer is between 20-25µm, making the overall coating thickness no more than 30µm, non-destructive measurement using the x-ray fluorescence (XRF) method is possible.

For this kind of application, x-ray fluorescence instruments with a proportional counter tube are perfectly suited. Even with small measurement spots, sufficiently high count rates can be obtained due to the large detector area, ensuring good repeatability precision. Because of the large, easily accessible measurement chamber, the robust instruments of the FISCHERSCOPE® X-RAY XDL® family are well suited for large specimens with complex shapes.

To maximize the precision of the results, proper positioning of the object is essential, for example by choosing an intrinsically horizontal area or correctly aligning the sample. To assist in this crucial step, FISCHERSCOPE® X-RAY measurement systems are equipped with a laser pointer as a positioning aid and high-magnification camera optics. Using the video image generated by the WinFTM® software, the required exact focusing of the measurement spot can be achieved.

Results of an X-Ray Measurement Using a FISCHERSCOPE® X-RAY XDL®

MEASUREMENT SPOT 1 2 3 4 5
Cr Mean Value 0.17 0.17 0.17 0.17 0.16
Standard Deviation 0.003 0.005 0.005 0.004 0.005
Ni Mean Value 7.24 7.4 7.1 7.29 7.21
Standard Deviation 0.07 0.04 0.10 0.11 0.07
Cu Mean Value 21.4 21.9 22.1 20.1 20.6
Standard Deviation 0.25 0.39 0.29 0.29 0.26

Typical results of an x-ray measurement, collected using a FISCHERSCOPE® X-RAY XDLM® with a measuring time of 30 seconds for four measurement cycles per spot.

Measure the Thickness of Decorative Cr/Ni/Cu Platings with Fischer

For determining the thickness of decorative Cr/Ni/Cu platings on plastic substrates with a maximum overall coating thickness of approximately 30µm, the cost-effective proportional counter tube measurement systems of the FISCHERSCOPE® X-RAY XDL® family are the optimal solution. To measure thicker coatings, instruments employing the (destructive) Coulometric method are also available as an alternative. For more information, please contact us below.

Microhardness of Dental Composites

In the last several years, great efforts have been made to replace amalgam fillings – which are fraught with disadvantages and therefore no longer used – with inlays made of modern composite resins. Because of the substantial challenges set by intensive daily use, these materials must be extremely durable and able to retain their shape. In order to verify a given composite’s suitability to this purpose, it is therefore necessary to determine precisely key mechanical properties such as micro-hardness and elasticity. Only then is it possible to guarantee optimal long-term results for the patient.

Hardness Measurement for the Analysis of Composite Fillings

Enticing snacks and beverages with high sugar and/or acid content are a constant temptation in today’s vast offering of fast and prepared foods. Even the best oral hygiene has trouble keeping up; often, the side effects of unhealthy eating habits are cavities. As a result, the removal of caries and the placement of fillings have become standard practices. However, the age of ugly black fillings is coming to an end, as tooth-coloured inlays and Onlays of composite resin are replacing their unsightly amalgam precursors.

Composite fillings are microscopic ceramic and glass particles set in a light-activated resin. Because the colour can be matched to existing natural teeth, they represent a significant cosmetic improvement over old amalgam fillings; nonetheless, they must still retain their shape and withstand the wear and stresses to which teeth are typically exposed. These are just the minimum suitability requirements for their use in dental repair work.

The demands placed on dental composites are, therefore relatively high: they must be able to guarantee a certain hardness, a certain elasticity, long-term stability in colour and form, as well as excellent adhesion to the healthy tooth material.

The micro-hardness and elasticity parameters (Young’s modulus) of the various, often nearly identical makeups of dental composites can be determined precisely and accurately using the FISCHERSCOPE® HM2000. Without extensive preparatory effort, samples can be placed into the HM2000 and measured; a few minutes later, the process is done. Using its high-precision sample stage, automated test sequences can be programmed to, for example, detect inhomogeneities in the composite material. Comparing “untreated” composites to samples exposed to e.g. acids, can provide the basis for deducing the filling’s ultimate durability in daily use. The HM2000’s high repeatability precision and extreme accuracy make it possible to see even the slightest differences.

FISCHERSCOPE® HM2000 Family.

Conclusion on Measuring the Microhardness of Dental Composites

With the FISCHERSCOPE® HM2000, mechanical properties such as micro-hardness and elasticity can be determined precisely for dental composite resins, allowing conclusions to be drawn about their imperviousness to the impacts of aggressive food substances. For further details please contact your FISCHER representative.

FISCHERSCOPE® HM2000 AND HM500 NANOINDENTERS

Explore Further

Automatic and manual stage Nanoindenters with the load range of 0-2,000mN

Detect Heavy Metals in Toys Using X-ray Fluorescence

Safety of Children’s Toys

Children’s toys contaminated with traces of heavy metals and other hazardous substances – sometimes in dangerously high concentrations – repeatedly make for alarming headlines. Thus, toy manufacturers are under considerable pressure to prove that their products are free of harmful substances so that they qualify for the appropriate safety labels.

Ensuring Safety of Children’s Toys

Within Europe, children’s toys are subject to both the toy safety directive and the standard DIN EN 71, which defines, for example, the criteria for testing mechanical and physical properties and organic compounds, electric toy safety, and the upper limits for certain heavy metals and other hazardous substances. This standard dictates that the object be exposed for one or two hours to 0.07 mol/l hydrochloric acid, which simulates gastric juices. The dissolved product is then analysed, usually with AAS or ICP. The disadvantages of this approach are that the sample is destroyed in the process and the tests are very time-consuming.

Analysis of hazardous substances in various toys using a FISCHERSCOPE® X-RAY XDV®-SDD.

Detection Limits for Various Plastics

In contrast, X-ray fluorescence (XRF) analysis is a straightforward method for the quick and non-destructive determination of the concentrations of Pb, Hg, Cd and other heavy metals. Table 1 shows the detection limits for various plastics measured with a FISCHERSCOPE® XDV®-SDD. In this way, the precise measurement results can be easily checked against the prescribed limiting values. Limiting values specified in DIN EN 71 and detection limits in ppm for three different plastic materials, as measured with a FISCHERSCOPE® XDV®-SDD. Average values are shown for a brown ABS sample (as well as standard deviations in brackets). The limiting values for Sb, As, Ba and Cr have been clearly exceeded.

ELEMENT LIMITING- VALUES DIN EN 71 DETECTION LIMITS MEASURING EXAMPLE ABS BROWN [STANDARD DEVIATION]
POM PVC ABS blue
Sb 60 42.6 43.2 24.9 45159 [180]
As 25 3.9 8.7 2.7 42 [3.8]
Ba 1000 138.0 87.0 60.0 2740 [79]
Cd 75 17.4 19.2 22.2 10 [8.4]
Pb 90 8.7 12.6 6.5 4 [4.3]
Hg 60 2.4 8.1 1.5 -3 [2.6]
Se 500 1.5 4.2 1.2 5 [1.7]
Cr 60 11.7 54.0 7.5 12134 [281]

Quick and Easy Determination of the Concentrations of Pb, Hg, Cd

Used as a screening method, the XRF warns the user if a given value has been exceeded. Further wet chemical analyses can then be carried out to crosscheck the result.

The pollutant concentration can also be measured very selectively, for example on the painted eye of a plastic figure. With the help of the XRF, an entire batch can be tested quickly, allowing the selective removal of individual contaminated parts – which might never have been detected in random tests. A further advantage is that the concentration of all heavy metals can be determined simultaneously in one measurement step.

The Right Measuring Device to Detect Hazardous Substances

With the FISCHERSCOPE® X-RAY XDV®-SDD, even the smallest concentrations of heavy metals and other hazardous substances in toys can be detected quickly and, above all, non-destructively. This makes it possible to verify compliance with specified regulations and standards. For further information please contact us by filling the form below.

HIGHLY POWERFUL EDXRF

Explore Further

Precise measurements of extremely thin coatings (as low as nanometers) on complex geometry small and large samples. Ideal for PCB & ROHS

Fischer Instrumentation (GB) open new Customer Applications & Support Centre

As part of its culture of Continuous Improvement, Fischer Instrumentation (GB), part of the global Helmut Fischer Group, set a plan to be more easily accessible for its customers and more centrally based in the UK, after being sited previously in the south of the country, in Hampshire.

The company has now completed a successful relocation to a new Customer Applications and Support Centre in Pershore, Worcestershire.

Darin Enefer, Fischer GB General Manager, explained more:

“We took the opportunity during the pandemic lockdown to step back from the business and make decisions that would help provide optimised customer service, whilst supporting our business growth ambitions.

We are pleased with our Pershore facility and welcome new and existing customers to discuss their measuring requirements and challenges, evaluate their materials and samples, try our range of measuring equipment, and participate in useful ‘hands-on’ learning workshops.”

The relocation has helped the company grow sales and this has been achieved through supporting clients in the Aerospace, Automotive, Engineering, Electronics and Precious Metals sectors, with high quality measuring solutions, supported by pro-active service and maintenance plans.

“We know from survey feedback how much our customers like collaborating with a supplier that has UK based service personnel, available parts, and country wide support. Customers can be supported on site or alternatively use our fully equipped Service Centre at Pershore.

We hope our new location will help to continue to support our customers and enable us to continue our current business uplift”

The Company

As a full-service supplier in the field of surface testing, Fischer has been developing instruments for non-destructive material analysis, coating thickness measurement and material testing since 1953.

Fischer offer a wide range of measuring devices for different industries: from simple handheld devices for quick testing on the go to fully integrated, high-end systems that automatically monitor your production.

Darin believes that the company is leading the way in terms of product quality and customer service.

“We have a high customer service orientation and a passion for helping the customer measure more accurately, more reliably, and efficiently. Our core values include Expertise and Passion, along with Trust and Commitment. These values help drive our behaviours and activities. The whole aim is to make our customer’s lives easier, underpinned by our Fischer mantra ‘‘Measuring Made Easy!”

The Benefits of Material Analysis and Measurement in the Aerospace Industry

Material analysis and measurement are vital parts of the manufacturing process for a wide range of industries, including the aerospace sector. These processes involve various instruments that test a component or material to determine certain aspects of its composition, such as conductivity or coating thickness. In the aerospace industry, some manufactured materials are so large that they require testing directly on the factory floor rather than in a lab environment. In these cases, handheld measurement instruments are especially effective.

Material composition analysis is essential for metal (such as aluminum or titanium alloys), coatings, and plastics in the aerospace industry. Data gathered can be used to make conclusions about the efficiency, safety, and performance of said materials, ensuring finalized products function reliably in demanding atmospheric conditions. These quality control procedures not only aid in certain safety measures, such as tin whisker prevention, but they also assist in reducing weight, increasing fuel efficiency, and more.

Nanoindentation For Aerospace Parts And Products

Nanoindentation is a type of material analysis that tests the hardness of coatings and solid surfaces. Unlike other traditional methods for testing hardness, this process measures multiple material characteristics. Specifically, it measures the elasticity and plastic capabilities of the material, including the indentation modulus, hardness, and creep. Nanoindentation is remarkably precise, as it measures materials down to the nanometer.

Manufacturers use specialized nanoindentation tools to test materials during the aerospace quality assurance process. These devices can perform tests at the particle level using cutting-edge nanotechnology. Some nanoindentation models, like the FISCHERSCOPE® HM2000, can perform additional tests, such as temperature fluctuations. This measurement is essential for determining the glass transition of aerospace plastics, which ensures a safer application. Additionally, the FISCHERSCOPE® HM2000 can test the durability of paint and galvanized coatings, as well as composite and gold-plated surfaces. These functions are essential for products like circuit boards that power aerospace equipment.

Material Analysis In Aerospace Manufacturing

From rocket launches to airline travel, the aerospace industry involves many high-stakes operations. This means that even the slightest flaw in a component can lead to a disaster, hence the need for highly reliable measurement technology.

At Fischer Technology, we specialize in developing instruments that provide precise, reliable measurements. For example, our FISCHERSCOPE® X-RAY XDL and XDLM models conduct easy, accurate analysis of parts regardless of their shape. These devices can also be automated to further streamline the quality assurance process. Additionally, they utilize energy dispersive X-ray fluorescence (XRF) spectrometers that provide non-destructive coating thickness measurements, thus protecting the integrity of the material. Similarly, the FISCHERSCOPE® X-RAY XDAL model also provides precise measurement but includes three different semiconductor detectors to meet various needs. The silicon PIN diode, for example, is ideal for measuring numerous materials across a large measuring area, while the silicon drift detector (SDD) offers improved energy resolution. These multiple options allow manufacturers to customize their testing process to fit their specific quality assurance procedure.

How Fischer Technology Can Help

Fischer Technology provides reliable testing instruments and systems that meet the rigorous demands of the aerospace industry. These options include nanoindentation tools, material analysis devices, and other equipment that measures a wide range of elements, such as hardness, composition, reactivity, and conductivity. Additionally, we offer a variety of handheld devices that are ideal for testing large-scale products while maintaining critical accuracy thresholds.

For more information about our products and how they can improve your quality assurance process, contact us today.

Comply with Standards for Coating Thickness Inside Storage Tanks

Anti-corrosion Coatings have Special Regulations

Anticorrosion coatings on the interior of storage tanks are critical when storing many types of products, whether saltwater or freshwater, gasoline, ballast, foamy liquids, or diesel. Typically, regulations are in place to ensure that the right coating is used. Quality inspection of the coating is an essential part of compliance with the regulations.

The Petrobras Standard is One of the Best Known

Although there are many such regulations, the Petrobras standard, N-1201:2008 – “Anticorrosion Coatings for the Interior of Storage Tanks”, is a good example. A multinational company headquartered in Brazil, Petrobras uses the above-mentioned standard wherever it has operations. This standard is in the public domain and can be accessed online from their database; it regulates all painting processes applied to storage tanks, from surface preparation, to painting and coating, through to final inspection.

Excerpt from the Petrobras Standard

Petrobras Standard Coating Types and Thicknesses

The Petrobras standard N-1201:2008 prescribes the following coating types and coating thicknesses for the different products to be stored, as listed in Table 1:

Coating Type 1:

  • Primer: one layer of epoxy-zinc phosphate paint: 100 µm
  • Top protective coating: two layers of non-solvent epoxy paint: 150 µm minimum thickness per layer.

Coating Type 2:

  • One layer of zinc-ethyl-silicate paint: 75 µm

Coating Type 3:

  • One layer of non-solvent epoxy resin, cured with polyamine
  • And embedded with ceramic or fiberglass: 800 µm

Single-handed measurements with the MP0R-FP.  The display is visible like a watch.

Easy Coating Thickness Measurement under Difficult Conditions

Once they are applied, the coatings need to be inspected – a tricky job, because this is done in place! The enormous tank still smells sharply of noxious paint fumes as a technician wearing bulky protective gear and a headlamp (perhaps the only source of light) is lowered into the slippery vessel to measure the coating thickness at a number of positions. And, since a normal handheld gauge with integrated probe will not work, as the tank geometry does not permit it in some spots, an external probe is necessary.

FISCHER developed the MP0x-FP products for just such applications performed under difficult conditions. While other thickness gauges on the market require the use of both hands (one to hold the instrument and the other for the probe), the wristband accessory is indispensable when the task itself requires some juggling.

Quick Coating Thickness Measurements with the MP0 and MP0R Series

Another very practical advantage of the MP0x-FP series is that calibration can be done outside the tank using FISCHER calibration accessories to maximise accuracy. This procedure only needs a piece of the original tank material, thus to avoid that the entire calibration procedure has to be performed directly in the tank.

The Right Choice with the MP0x-FP Series Coating Thickness Gauges from Fischer

Besides the unmatched accuracy and repeatability performance of the MP0x-FP series from FISCHER, extra features like the wristband or the easy calibration process make these coating thickness gauges the ideal choice for checking compliance with regulations like the Petrobras standard N-1201:2008 for storage tanks. Handheld devices for simple coating thickness measurements in harsh environments.

For more information, please contact your local FISCHER representative:

FISCHER INSTRUMENTATION (GB) LTD – 12 Goodwood Road, Keytec 7 Business Park, Pershore, Worcestershire, WR10 2JL.

Telephone:  +44 (0) 1386 577370

Or visit: www.fischerinstrumentation.co.uk